Cool DIY Vacuum Tube Video

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John Futter
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Re: Cool DIY Vacuum Tube Video

Post by John Futter » Thu Jul 10, 2008 6:57 am

Steven
From my earlier training as an instrument maker 30 odd years ago I did as part of it 3 months of scientific glass blowing.
depends on what glass the final is but an intermediate with differing thermal expansion is required between the tungsten wire and the final glass or is it Kovar wire which would require a different intermediate.
From memory platinum wire is compatible with pyrex directly-- or was it soda glass or quartz

don't quote me

for the first time in thirty years I did a little glass bending 3 months ago to make some annealing supports for our substrates in the vacuum furnace for annealling at 600 degrees, made of pyrex.


ruined a few days later by the students who thought it was made of quartz and took it to 1000 degrees celsius melting it to the furnace quartz tube which imploded during cooldown because of the differing thermal expansions.

I'll go and talk to the glass blower next week and find out about it and if he has any.

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Richard Hull
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Re: Cool DIY Vacuum Tube Video

Post by Richard Hull » Thu Jul 10, 2008 2:45 pm

A useful tip relates to sealing electrodes to glass.

Platinum is compatible with most all glass as is, provided it is of small diameter.

Likewise, very thin tunsten welding rod is also useable with glasses, but it has to be treated with sodium nitrite at high temps. .010 rod stock is good. Tim Raney of our group here does this a lot. Tim now tends to use the classic graded seal using small dabs of uranium glass beads.

U glass is readily found on larger used hydrogen thyratrons and other large vacuum tubes at hamfests. Smash them and either keep the graded seal or just the U glass.

Cheaper still might be vaseline glassware. I haven't tried it yet as a graded seal, but about $40.00 will get you a large item from an antique store that would make thosuands of such seals. The U glass marbles that used to be on ebay might serve also.

Graded seals are real pretty and can take a good deal of heating (expansion and contraction without failure as witnessed in the old glass H2 thyratrons that run really hot. Some number to look for 4C35, 5C22. The 5C22 is still avaialble commercially for $1195.000. I found two at a recent hamfest of $2.00 each.

Richard Hull
Progress may have been a good thing once, but it just went on too long. - Yogi Berra
Fusion is the energy of the future....and it always will be
Retired now...Doing only what I want and not what I should...every day is a saturday.

DaveC
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Re: Cool DIY Vacuum Tube Video

Post by DaveC » Thu Jul 10, 2008 6:44 pm

The standard metals for inexpensive glass feedthroughs are Kovar and Dumet which more or less match the thermal expansion of soft glasses. As Richard notes small diameter Tungsten is also a close match for soft glass seals, as is Patinum. As I recall, the key is to have a wettable outer surface for the wire lead. For Tungsten, this is some sort of oxide.

Rosebury' Book on Vacuum Tube materials and Techniques, has some useful tables of thermal expansion for various glasses as well as the metal types the match reasonably well.

One reasonably good source for feedthrough stock, is any discarded incandescent bulb. Not sure how good a seal this is for extended high vac applications, but definitely works for about 1000 hrs more or less.

I think, you can still buy graded seals, but can't remember where... sorry... But the price is a lot more than that of a stray U glass jar from a junk shop. A lead borate glass is routinely used in CRT e-gun bases.

Dave Cooper

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Re: Cool DIY Vacuum Tube Video

Post by teslacoil.it » Tue Jul 15, 2008 4:41 pm

I recently played with glass.


After some research, i found a great source of cheap dumet wire that match with neon signs manufacturing glass tubes........ many small diodes (eg 1N4148 or some zeners if bigger terminals are needed) are made with glass; just wipe terminals with sandpaper to remove tin/lead layer and you are ready to play with glass!


i attach some pics of my creations, please note, i'm NOT a real glass blower, i'm just play with some glass, flames and vacuum!

http://img213.imageshack.us/img213/3345/tubows4.jpg
http://img442.imageshack.us/img442/4971 ... odoyk7.jpg
http://img209.imageshack.us/img209/1269 ... uranl4.jpg

http://img444.imageshack.us/img444/8743 ... adeoy1.jpg
http://img205.imageshack.us/img205/2734 ... do2py2.jpg



Equipment used:

some torches
http://img241.imageshack.us/img241/858/fiammeco8.jpg

anealing oven
http://img329.imageshack.us/img329/4391 ... 30cxm0.jpg

Spotwelder
http://img364.imageshack.us/img364/1323 ... ce1hf2.jpg

some spotwelded items!
http://img88.imageshack.us/img88/1606/e ... aticz4.jpg
http://img216.imageshack.us/img216/5540/puntataiu7.jpg
http://img257.imageshack.us/img257/5877/geogrid1jn4.jpg
http://img443.imageshack.us/img443/2739/geogrid2od4.jpg


Little off topic here...... my new fusor chamber!
http://img217.imageshack.us/img217/6510/iosferaip4.jpg


Ciao!
Fabio!

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Steven Sesselmann
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Re: Cool DIY Vacuum Tube Video

Post by Steven Sesselmann » Wed Jul 16, 2008 3:04 am

Fabio,

Nice setup, I am impressed!

Have you considered building a sealed glass fusor?

Steven
http://www.gammaspectacular.com - Gamma Spectrometry Systems
https://www.researchgate.net/profile/Steven_Sesselmann - Various papers and patents on RG

teslacoil.it
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Re: Cool DIY Vacuum Tube Video

Post by teslacoil.it » Wed Jul 16, 2008 11:18 am

YES of course!

But these tubes are my really first glass works with positive results, actually i haven't neither the skill nor the material/equipment required to blow a larger tube, generally the glass crack during the cooling down defeating all the work!

anyhow, work in progress, i recovered some unused getters, these are able to achieve high degrees of vacuum inside of a permanently sealed tube even with a simple dual stage pump; a sealed-glass fusor (deuterium filled!) will made when i'll be able to achieve it.

Ciao!
Fabio.

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